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- W2076809367 abstract "Experimental details describing the addition of CF3OF to hexa-O-accetyl-D-lactal (I) are presented. Four fluorinated disaccharides: trifluoromethyl 3,6-di-O-acetyl-2-fluoro-4-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-mannopyrinoside (V), trifluoromethyl 3,6-di- O-acetyl-2-deoxy-2-fluoro-4-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranoside (VI), 3,6-di-O-acetyl-2-deoxy-2-fluoro-4-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-mannopyranosyl fluoride (VII), and 3,6-di-O-acetyl-2-deoxy-2-fluoro-4-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl fluoride (VIII) were isolated from the product mixture. The profound changes in both the rate and the major products of the addition, compared to those reported for related monosaccharide glycals, are discussed in relation to the steric influence exerted by the presence of the non-reducing (galactoside-B) ring of the disacchride glycals. The configuration and the confirmation of the fluorinated portion of the adducts were assigned on the basis of 19F.m.r. spectroscopic parameters and the structural" @default.
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- W2076809367 date "1977-12-01" @default.
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- W2076809367 title "Fluorocarbohydrates Part XXV. Synthesis and structure of 2-deoxy-2-fluorolactose and related compounds" @default.
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- W2076809367 doi "https://doi.org/10.1016/s0022-1139(00)82427-6" @default.
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