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- W2076809625 abstract "The synthesis of metals and alloys by mechanochemical reduction of their oxides is a recent extension of the mechanical alloying process. The materials used in this study were CuO (AJAX, AR grade, 5--110[mu]m) and graphite (CERAC, 99.4%, 150--420[mu]m). Milling was carried out in a Spex 8000 mixer/mill using a hardened steel vial and ten 12.7-mm-diameter hardened steel balls. A ball-to-powder mass ratio of 12:1 was employed in all tests. X-ray measurements showed that the reduction of CuO occurred via a two-stage CuO [r arrow] Cu[sub 2]O [r arrow] Cu, process. The amount of CuO decreased monotonically during milling. The increase in the rate of CuO reduction during the initial stage of milling is consistent with the effect of microstructural refinement on reaction kinetics. The amount of Cu[sub 2]O reached a maximum of [approximately]45 wt% after 9 hours of milling and subsequently decreased to zero after 24 hours. The initial increase in amount of Cu[sub 2]O is associated with the relatively high reduction rate of CuO whereas, the subsequent decrease in Cu[sub 2]O resulted from the formation of Cu." @default.
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- W2076809625 date "1995-03-01" @default.
- W2076809625 modified "2023-10-06" @default.
- W2076809625 title "Mechanochemical reduction of CuO by graphite" @default.
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- W2076809625 doi "https://doi.org/10.1016/0956-716x(95)91585-d" @default.
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