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- W2076892025 abstract "An on-line procedure has been developed and validated for the clean-up and fractionation of ortho and non-ortho-PCBs in fruit and vegetable samples. The procedure combines silica/acid and carbon/glass fibre columns with gas chromatography-mass spectrometry. Chromatography on carbon/glass fibre allowed collection of mono-ortho/di-ortho and non-ortho-PCB fractions, which were determined separately by GC-MS. The method was validated by replicate analyses and by inter-laboratory comparison of data for PCB congeners determined in fruit and vegetable samples collected in South Wales. The concurrent determination of ortho and non-ortho substituted PCBs is reported with recoveries ranging from 55-95% and a mean intra-laboratory precision (%COV) of 9.5% for apple extracts." @default.
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- W2076892025 date "1997-10-01" @default.
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- W2076892025 title "Validation of a congener specific method for Ortho and non-Ortho substituted polychlorinated biphenyls in fruit and vegetable samples" @default.
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- W2076892025 doi "https://doi.org/10.1016/s0045-6535(97)00235-x" @default.
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