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- W2076996522 abstract "A gas-liquid chromatographic procedure permitting rapid analysis of the major fatty acids commonly found in vegetable oils was evaluated with standards of known composition and found to be both accurate and precise. A standard containing 20% by weight of each of the methyl esters of palmitic, stearic, oleic, linoleic, and linolenic acid was analyzed in 2.7 min with errors of 1.6, 0.7, 3.3, 0.8, and 3.1%, respectively. Six procedures, requiring from 2.7 to 25 min for the eluation of the effects of the operational parameters, carrier gas flow rate and column temperature, on the precision and accuracy of gasliquid chromatographic analysis of fatty acid methyl esters. The most rapid procedure, obtained with a column temperature of 235C and a helium flow rate of 110 ml/min was found to be comparable in accuracy and precision to the other procedures and gave quantitative results with National Heart Institute type fatty acid standards KA, KB, and KD, that agreed with stated composition with a relative error of less than 2% for major components (10% or more of total mixture) and less than 6% for minor components (less than 10% of total mixture)." @default.
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- W2076996522 date "1966-12-01" @default.
- W2076996522 modified "2023-10-05" @default.
- W2076996522 title "Rapid gas-liquid chromatographic procedure for the analysis of methyl esters of long chain fatty acids" @default.
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- W2076996522 doi "https://doi.org/10.1007/bf02682565" @default.
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