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- W2077131628 abstract "This letter describes the chemical synthesis of highly mono-dispersed spherical nano-PbO2. In the first step, sodium borohydride in the presence of TritonX-100 was used to reduce Pb(NO3)2 to highly spherical nano-Pb, and the second NaOCl was used to oxidize nano-Pb to nano-PbO2 (both reactions were performed at room temperature). TEM, SEM, XRD, and XPS surface analyses showed that the prepared Pb and PbO2 particles were spherical, 95% were mono-dispersed and of the size of 30 nm. In addition, electrochemical active surface area studies confirmed the nano-particulate nature of the prepared PbO2 particles. The developed procedure is straightforward, rapid, performed at room temperature, and scalable to the industrial level." @default.
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- W2077131628 date "2014-05-01" @default.
- W2077131628 modified "2023-10-16" @default.
- W2077131628 title "Controlled synthesis of highly spherical nano-PbO2 particles and their characterization" @default.
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- W2077131628 doi "https://doi.org/10.1016/j.matlet.2014.02.083" @default.
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