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- W2077180573 abstract "Abstract The technique of fast magic-angle specimen rotation has been used to substantially reduce the width of the nuclear magnetic resonance spectra of 27Al, 111Cd, and 113Cd in pure aluminium and cadmium. Rotation at 8 kHz reduced the width of the 27Al line from 9 kHz to 400 Hz which facilitated an accurate determination of the Knight shift. Relative to an aqueous solution of AICl3, the Knight shift was found to be 1640 ± 1ppm. Rapid rotation removed the large anisotropic Knight shift present in both isotopes of cadmium and left narrow lines with widths determined by lifetime broadening and the indirect electron-coupled nuclear interaction. Experimental values for the isotropic Knight shifts of cadmium are 4321 ± 7 and 4324 ± 7 ppm for 111Cd and 113Cd, respectively, relative to an aqueous solution of cadmium nitrate." @default.
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- W2077180573 date "1974-08-01" @default.
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- W2077180573 title "NMR in rapidly rotated metallic aluminium and cadmium" @default.
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- W2077180573 doi "https://doi.org/10.1016/0022-2364(74)90070-5" @default.
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