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- W2077321404 abstract "15N n.m.r. spectra of [13C-2, 3-15N2-guanidino]arginine and [13C, 15N2] urea were obtained in D2O and H2O at a variety of pH values both with and without proton decoupling. The effects of the proton exchange rate are readily observable in the proton coupled 15N spectra. When the guanidino group is deprotonated (pK = 12.5), the terminal nitrogens give a single resonance 6.6 ppm downfield of the protonated species, indicating a rapid tautomeric exchange. The observed NH and CN couplings are compared with calculated values, and good agreement is found for 1J(CN) using a Blizzard–Santry type calculation. The ramifications of the proton exchange on 15N n.m.r. spectra of amino acids and peptides are discussed." @default.
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- W2077321404 date "1977-10-01" @default.
- W2077321404 modified "2023-10-13" @default.
- W2077321404 title "Nitrogen-15 n.m.r. studies of13C,15N labeled arginine" @default.
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- W2077321404 doi "https://doi.org/10.1002/mrc.1270091011" @default.
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