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- W2077516854 abstract "Abstract A series of 15 N-labeled 6-amino-6-deoxy-1,2:3,5-di- O -isopropylidene-α- d -glucofuranose derivatives and their 14 N analogs has been studied by continuous-wave proton, 13 C, and 19 F magnetic resonance spectroscopy, and by 13 C Fourier-transform techniques. Characteristic chemical shifts and the magnitudes of 1 H 1 H, 1 H 15 N, 1 H 19 F, 13 C 15 N, and 15 N 19 F coupling-constants are reported and discussed. The 1 H 15 N and 13 C 15 N coupling-constants over one bond have been used to assess the hybridization of the 15 N atom in three of the derivatives. Heteronuclear, internuclear, double-resonance (indor 1 ) and triple-resonance (“intripler”) experiments have been performed in which 15 NH proton transitions were monitored while the 15 N or 19 F frequencies were swept or maintained on resonance. Replicas of the computed, theoretical 15 N spectrum were recorded indirectly, and are discussed in relation to nuclear Overhauser effects." @default.
- W2077516854 created "2016-06-24" @default.
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- W2077516854 date "1971-11-01" @default.
- W2077516854 modified "2023-09-24" @default.
- W2077516854 title "The n.m.r. spectroscopy of derivatives of 6-amino-6-deoxy-d-glucose-6-15N. 13C Fourier-transform and internuclear, double- and triple-resonance studies" @default.
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- W2077516854 doi "https://doi.org/10.1016/s0008-6215(00)84953-8" @default.
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