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- W2077523770 abstract "Abstract The crystallization of a melt spun amorphous Al based alloy (Al70Fe13Si17) has been studied by various techniques. In situ Transmission Electon Microscopy (TEM) combined with Scanning Transmission Electron Microscope microanalysis (STEM) and high resolution TEM provide most of the information on the crystallization sequences, while their representativity and kinetics are controlled and precised by “bulk” techniques [Scanning Electron Microscopy (SEM), Differential Scanning Calorimetry (DSC) and Small Angle X-ray Scattering (SAXS)]. The crystallization occurs in two steps: it first appears a very small volume fraction of tiny Al particles (less than 2%) before the complete crystallization of the metallic glass in two intermetallic compounds (called β and τ4). Both phases β and τ4 are in epitaxy and form a multisliced sandwich. On about 0.25 nm2 surface microanalyses, the global composition of β + τ4 containing Al particles corresponds to the initial glass composition. By in situ annealing of electropolished Al70Fe13Si17 amorphous samples, another crystallization occurs just within the thin parts of samples: a phase called α or τ5 surrounded by aluminium. Such transformation can be considered as an artefact; nevertheless its study related to crystallographic studies has represented the basis of another work aimed to a structural modelling of the AlMn and AlFe quasicristalline phases." @default.
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- W2077523770 date "1986-09-01" @default.
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- W2077523770 title "Crystallization study of the melt spun Al70Fe13Si17 glass" @default.
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- W2077523770 doi "https://doi.org/10.1016/0001-6160(86)90122-7" @default.
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