Matches in SemOpenAlex for { <https://semopenalex.org/work/W2077542431> ?p ?o ?g. }
Showing items 1 to 83 of
83
with 100 items per page.
- W2077542431 endingPage "608" @default.
- W2077542431 startingPage "601" @default.
- W2077542431 abstract "A new extraction method for 12 sulfonamides (sulfadiazine, sulfathiazole, sulfapyridine, sulfamerazine, sulfamethizole, sulfadimidine, sulfisoxazole, sulfamethoxazole, sulfatroxazole, sulfachlorpyrazine, sulfaphenazole and dapsone) in muscle, liver and kidney was developed. Fortified tissues of muscle, liver and kidney from bovine, pig and chicken were studied. A 10 g tissue and 10 ml acetonitrile were homogenised with an Ultra-Turrax. Next, the tissue was defatted with 5 ml n-hexane, centrifuged and filtered into flasks. Then the extracts were acidified with 10 ml hydrochloric acid and diluted with deionised water. Next, the samples were loaded on OASIS® MCX columns, which were conditioned with 5 ml methanol and 5 ml water. The columns were washed with 5 ml hydrochloric acid and 5 ml methanol. Then the samples were eluted with 5 ml ammonia solution/acetonitrile (v/v 1/19), allowed to dry under nitrogen and reconstituted in 200 μl acetonitrile/water-mixture (v/v 1/4). The analyses were carried out on HPLC–DAD. Mobile phase was 0.01 M ammonium acetate pH 4.6 (A) and acetonitrile (B). Chromatographic separation was obtained by gradient elution (5% B to 40% within 16 min, back to 5% in 1 min, equilibration for 3 min). The sulfonamides were detected at 260 nm and dapsone at 294 nm. The detection limits of the HPLC method were 1 ppb for all analytes." @default.
- W2077542431 created "2016-06-24" @default.
- W2077542431 creator A5067408274 @default.
- W2077542431 date "2003-12-01" @default.
- W2077542431 modified "2023-10-16" @default.
- W2077542431 title "Determination of sulfonamides in animal tissues using cation exchange reversed phase sorbent for sample cleanup and HPLC–DAD for detection" @default.
- W2077542431 cites W134366744 @default.
- W2077542431 cites W1972421892 @default.
- W2077542431 cites W2068460154 @default.
- W2077542431 cites W2168064352 @default.
- W2077542431 doi "https://doi.org/10.1016/s0308-8146(03)00254-1" @default.
- W2077542431 hasPublicationYear "2003" @default.
- W2077542431 type Work @default.
- W2077542431 sameAs 2077542431 @default.
- W2077542431 citedByCount "52" @default.
- W2077542431 countsByYear W20775424312012 @default.
- W2077542431 countsByYear W20775424312013 @default.
- W2077542431 countsByYear W20775424312014 @default.
- W2077542431 countsByYear W20775424312015 @default.
- W2077542431 countsByYear W20775424312016 @default.
- W2077542431 countsByYear W20775424312017 @default.
- W2077542431 countsByYear W20775424312018 @default.
- W2077542431 countsByYear W20775424312019 @default.
- W2077542431 countsByYear W20775424312020 @default.
- W2077542431 countsByYear W20775424312021 @default.
- W2077542431 countsByYear W20775424312023 @default.
- W2077542431 crossrefType "journal-article" @default.
- W2077542431 hasAuthorship W2077542431A5067408274 @default.
- W2077542431 hasConcept C119128265 @default.
- W2077542431 hasConcept C178790620 @default.
- W2077542431 hasConcept C179998833 @default.
- W2077542431 hasConcept C185592680 @default.
- W2077542431 hasConcept C2776377007 @default.
- W2077542431 hasConcept C2777436746 @default.
- W2077542431 hasConcept C2777463227 @default.
- W2077542431 hasConcept C2777990680 @default.
- W2077542431 hasConcept C2778269047 @default.
- W2077542431 hasConcept C2779056493 @default.
- W2077542431 hasConcept C2779607525 @default.
- W2077542431 hasConcept C2780599964 @default.
- W2077542431 hasConcept C43617362 @default.
- W2077542431 hasConcept C4725764 @default.
- W2077542431 hasConcept C501593827 @default.
- W2077542431 hasConcept C55493867 @default.
- W2077542431 hasConcept C73826308 @default.
- W2077542431 hasConceptScore W2077542431C119128265 @default.
- W2077542431 hasConceptScore W2077542431C178790620 @default.
- W2077542431 hasConceptScore W2077542431C179998833 @default.
- W2077542431 hasConceptScore W2077542431C185592680 @default.
- W2077542431 hasConceptScore W2077542431C2776377007 @default.
- W2077542431 hasConceptScore W2077542431C2777436746 @default.
- W2077542431 hasConceptScore W2077542431C2777463227 @default.
- W2077542431 hasConceptScore W2077542431C2777990680 @default.
- W2077542431 hasConceptScore W2077542431C2778269047 @default.
- W2077542431 hasConceptScore W2077542431C2779056493 @default.
- W2077542431 hasConceptScore W2077542431C2779607525 @default.
- W2077542431 hasConceptScore W2077542431C2780599964 @default.
- W2077542431 hasConceptScore W2077542431C43617362 @default.
- W2077542431 hasConceptScore W2077542431C4725764 @default.
- W2077542431 hasConceptScore W2077542431C501593827 @default.
- W2077542431 hasConceptScore W2077542431C55493867 @default.
- W2077542431 hasConceptScore W2077542431C73826308 @default.
- W2077542431 hasIssue "4" @default.
- W2077542431 hasLocation W20775424311 @default.
- W2077542431 hasOpenAccess W2077542431 @default.
- W2077542431 hasPrimaryLocation W20775424311 @default.
- W2077542431 hasRelatedWork W1898302256 @default.
- W2077542431 hasRelatedWork W1989562735 @default.
- W2077542431 hasRelatedWork W1992749909 @default.
- W2077542431 hasRelatedWork W2036693590 @default.
- W2077542431 hasRelatedWork W2047065357 @default.
- W2077542431 hasRelatedWork W2077815983 @default.
- W2077542431 hasRelatedWork W2094705122 @default.
- W2077542431 hasRelatedWork W2127889175 @default.
- W2077542431 hasRelatedWork W2571147792 @default.
- W2077542431 hasRelatedWork W4233243371 @default.
- W2077542431 hasVolume "83" @default.
- W2077542431 isParatext "false" @default.
- W2077542431 isRetracted "false" @default.
- W2077542431 magId "2077542431" @default.
- W2077542431 workType "article" @default.