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- W2077543514 abstract "Dynamic secondary-ion mass spectrometry (SIMS) was used to measure equilibrium volume-fraction profiles of a symmetric diblock copolymer at a polymer/polymer interface. The three polymers were a saturated polybutadiene with 90% 1,2-addition (sPB90) homopolymer, a saturated polybutadiene with 63% 1,2-addition (sPB63) homopolymer, and a sPB90−sPB63 diblock copolymer. The molecular weights of the homopolymers were chosen such that the sPB90/sPB63 blend was deep in the two-phase region. The experimentally determined volume-fraction profiles were compared with self-consistent-field theory calculations (SCFT). The statistical segment lengths and the Flory−Huggins interaction parameter were obtained independently from small-angle neutron scattering (SANS) measurements on a low molecular weight, homogeneous binary sPB90/sPB63 blend. Thus, no adjustable parameters were used in the SCFT calculations. Adsorption isotherms and the measured diblock copolymer volume-fraction profiles are in excellent agreement with the SCFT calculations. This work demonstrates that Flory−Huggins interaction parameters and statistical segment lengths determined by SANS can be used to predict complex phase behavior, including interfacial adsorption of block copolymers." @default.
- W2077543514 created "2016-06-24" @default.
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- W2077543514 date "2005-04-09" @default.
- W2077543514 modified "2023-09-27" @default.
- W2077543514 title "Experimental and Theoretical Study of the Adsorption of a Diblock Copolymer to Interfaces between Two Homopolymers" @default.
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- W2077543514 doi "https://doi.org/10.1021/ma047539s" @default.
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