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- W2077624134 abstract "A series of carbonyl derivatives of 5-imino-Δ3-1,2,4-thiadiazolines has been prepared and shown by X-ray analysis of a selected example to have a trithiapentalene-like structure. When diphenylketene was used as acylating reagent, the primary product (14), obtained at room temperature, rearranged on heating in a polar solvent into a Δ2-thiazolin-4-one (15). The structure of 15 has been confirmed by X-ray analysis, and shown to be a zwitterion. Rearranged products (i.e., 16 and 20-22) were also obtained when 3 was reacted with dimethyl acetylenedicarboxylate or methanesulfonyl chloride, whereas tosyl chloride gave normal tosylated derivatives (17-19). The latter have also a nearly linear N-S…O arrangement, but the interaction between S and O is weak." @default.
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- W2077624134 date "1981-11-01" @default.
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- W2077624134 title "5-Imino-Δ<sup>3</sup>-1,2,4-thiadiazoline derivatives with a linear N-S…O grouping. Synthesis and crystal structures" @default.
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- W2077624134 doi "https://doi.org/10.1002/jhet.5570180708" @default.
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