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• W2077650551 endingPage "8193" @default.
• W2077650551 startingPage "8188" @default.
• W2077650551 abstract "Crystalline samples of rare earth carbodiimides were synthesized by solid-state metathesis reactions of rare earth trichlorides with lithium cyanamide in sealed silica ampules. Two distinct structures were determined by single-crystal X-ray diffraction. The structure determined for Sm2(CN2)3 [C2/m, Z = 2, a = 14.534(2) Å, b = 3.8880(8) Å, c = 5.2691(9) Å, β = 95.96(2)°, R1 = 0.0267, and wR2 = 0.0667] was assigned for RE2(CN2)3 compounds with RE = Y, Pr, Nd, Sm, Gd, Tb, Dy, Ho, and Er, and the structure determined for Lu2(CN2)3 [R32, Z = 3, a = 6.2732(8) Å, c = 14.681(2) Å, R1 = 0.0208, and wR2 = 0.0526] was assigned for the smallest rare earth ions with RE = Tm, Yb, and Lu by powder X-ray diffraction. Both types of crystal structures are characterized by layers of [NCN]2- ions whose arrangements can be derived from the motif of a closest packed layer of sticks. These layers alternate with layers of rare earth ions in a one-by-one sequence. Different tilting arrangements of the N−C−N-axes relative to the stacking directions (c) and different arrangements of RE3+ ions within metal atom layers account for the two distinct structures in which Sm3+ and Lu3+ ions adopt the coordination numbers 7 and 6, respectively." @default.
• W2077650551 created "2016-06-24" @default.
• W2077650551 creator A5043775825 @default.
• W2077650551 creator A5060590117 @default.
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• W2077650551 date "2006-09-07" @default.
• W2077650551 modified "2023-10-15" @default.
• W2077650551 title "Syntheses and Structural Properties of Rare Earth Carbodiimides" @default.
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• W2077650551 doi "https://doi.org/10.1021/ic0608952" @default.
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