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- W2077773634 abstract "The reaction of 1,1-dimethyl-2,5-diphenyl-1-silacyclohexa-2,4-diene with iron pentacarbonyl or diironnonacarbonyl gave a mixture of tricarbonyl(1,1-dimethyl-2,5-diphenyl-1-silacyclohexa-2,4-diene)iron and tricarbonyl(1,1-dimethyl-3,6-diphenyl-1-silacyclohexa-2,4-diene)iron. Similarly, on treatment with iron pentacarbonyl 1,1-dimethyl-2,5-diphenyl-4-trimethylsilyl-1-silacyclohexa-2,5-diene yielded a mixture of tricarbonyl-(1,1-dimethyl-3,6-diphenyl-4-trimethylsilyl-1-silacyclohexa-2,4-diene)iron, tricarbonyl(1,1-dimethyl-2,5-diphenyl-4-trimethylsilyl-1-silacyclohexa-2,4-diene)iron, and tricarbonyl(1,1-dimethyl-2,5-diphenyl-6-trimethylsilyl-1-silacyclohexa-2,4-diene)iron as a result of migration of the hydrogen on the ligand competing with silyl migration. On thermolysis, 1,1-dimethyl-2,5-diphenyl-4-trimethylsilyl-1-silacyclohexa-2,5-diene underwent only 1,3-silyl-migration to yield 1,1-dimethyl-2,5-diphenyl-6-trimethylsilyl-1-silacyclohexa-2,4-diene. The mechanism of transition-metal assisted hydrogen-migration is discussed." @default.
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- W2077773634 date "1986-05-01" @default.
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- W2077773634 title "Preparations and Thermal Isomerization of Some Tricarbonyl(1-silacyclohexadiene) Iron Complexes. Silyl and Hydrogen Migration in the Diene and the Diene Complex" @default.
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- W2077773634 doi "https://doi.org/10.1246/bcsj.59.1509" @default.
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