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• W2077853818 endingPage "1190" @default.
• W2077853818 startingPage "1187" @default.
• W2077853818 abstract "Tin-119 NMR spectral studies in the solid state and in solution of [Sn2R4] (R = C6HBut-2-Me3-4,5,6) 3 are presented. The ambient temperature 119Sn CP-MAS NMR spectrum displayed a single resonance at δiso 819, while variable-temperature spectra in toluene clearly indicated the existence of a rapid equilibrium between the loosely held dimer 3 and its monomer SnR2. Photolysis of either 3 or its digermanium analogue in benzene yielded the persistent radicals [MR3]˙ (M = Ge or Sn), which were studied by ESR spectroscopy. The ESR parameters are compared with other trialkyl- and triamido-tin(III)- and -germanium(III)-centred radicals. Noteworthy is the first observation of 13C hyperfine coupling for a Group 14 metal-centred radical, 18(1) G for [SnR3]˙ and 10(1) G for [GeR3]˙." @default.
• W2077853818 created "2016-06-24" @default.
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• W2077853818 date "1998-01-01" @default.
• W2077853818 modified "2023-09-24" @default.
• W2077853818 title "Magnetic resonance spectroscopic studies of a tetraaryl-distannene and -digermene [M2R4] (R = C6HBut-2-Me3-4,5,6 and M = Sn or Ge) †" @default.
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• W2077853818 doi "https://doi.org/10.1039/a709141i" @default.
• W2077853818 hasPublicationYear "1998" @default.
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