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• W2077885853 abstract "The combination of glass capillary gas chromatography--mass spectrometry is especially suitable for the recognition of compounds. The use of [3,4-13C]testosterone as internal standard, mass fragmentography and isotope ratio measurement have been applied to the quantitative determination of testosterone in plasma. This paper describes the method, using tert.-butyldimethylsilylmethoxime and di-heptafluorobutyrate derivatives. The calibration graph in isotopic dilution is examined. The results obtained are compared with the results obtained by radioimmunoassay. The sensitivity of the method is judged from the lower limit of detection: 4.5 pg. The precision, and inter- and intra-assay are calculated." @default.
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• W2077885853 date "1985-01-01" @default.
• W2077885853 modified "2023-09-23" @default.
• W2077885853 title "Determination of plasma testosterone by mass fragmentography using [3,4-13C]testosterone as an internal standard" @default.
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• W2077885853 doi "https://doi.org/10.1016/s0378-4347(00)84650-2" @default.
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