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- W2077887218 abstract "The isomerization of readily available allyl ethers catalyzed by soluble ruthenium complexes is an extremely versatile methodology for synthesis of O-1-propenyl systems—attractive monomers in cationic UV-radiation curing technology. From the process development perspective, the effectiveness of selected simple ruthenium catalyst precursors, mainly [RuClH(CO)(PPh3)3], [RuCl2(PPh3)3] and RuCl3·xH2O in the solvent-free isomerization of 1,4-bisallyloxybutane has been examined. The relationship between basic reaction parameters such as the reaction temperature, the amount of catalyst precursor, the promoters of non-hydride complexes (bases or alcohols), the ambient gas atmosphere and the reaction time allowing to achieve quantitative conversion of the model bisallyl ether to its 1-propenyl derivatives (τ100%) has been presented. Particular attention has been paid to the use of lower loadings of [Ru] complex required for the completion of the reaction within the reasonable times. For the first time a detailed study on the effect of the presence and amount of allyl hydroperoxides on the course of isomerization has been done." @default.
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- W2077887218 date "1976-01-01" @default.
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- W2077887218 title "On the existence of dioxygen adducts of ruthenium (II) tertiary-arsine and -phosphine complexes" @default.
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- W2077887218 doi "https://doi.org/10.1016/s0020-1693(00)94065-9" @default.
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