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• W2077896582 abstract "The first catalytic cross-metathesis reaction of an alkyne with a nitrile is described. The nitride complex N⋮W(OC(CF3)2CH3)3(DME) undergoes reversible triple-bond metathesis reactions with alkynes (RC⋮CR; R = Et, 4-C6H4OMe), forming the alkylidyne complexes RC⋮W(OC(CF3)2CH3)3(DME) (R = Et, 4-C6H4OMe) along with the corresponding nitrile RC⋮N. This has been exploited to effect catalytic cross-metathesis of nitriles with alkynes, in which the organic CR fragments of two nitriles are coupled to yield an alkyne. A simple “sacrificial” alkyne (3-hexyne) acts as the N-atom acceptor, forming two equivalents of nitrile byproduct (propionitrile)." @default.
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• W2077896582 date "2007-03-14" @default.
• W2077896582 modified "2023-10-09" @default.
• W2077896582 title "Catalytic Nitrile-Alkyne Cross-Metathesis" @default.
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• W2077896582 doi "https://doi.org/10.1021/ja0693439" @default.
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