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- W2077982059 abstract "Abstract A series of catalyst containing 20–70% of 12-tungstosilicicacid (TSA) supported onto neutral alumina (A) has been synthesized, characterized and evaluated for esterification of 1° and 2° alcohols. The best catalyst, TSA 3 /A (30% loading of 12-tungstosilicicacid onto neutral alumina) has been compared with TSA 3 /Z (30% loading of 12-tungstosilicicacid onto hydrous zirconia) in order to see the effect of nature of support. The catalytic activity of TSA 3 /A and TSA 3 /Z has also been explored for tert -butylation of phenol by varying different parameters. Both the catalysts were calcined in the temperature range of 300–500 °C and characterized by FT-IR, DRS and XRD to see the structural change in the calcined materials. Their catalytic activity was also evaluated for the esterification as well as tert -butylation of phenol under optimized conditions. An attempt has also been made to regenerate and to reuse the present catalysts, especially for tert -butylation of phenol." @default.
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- W2077982059 date "2007-09-01" @default.
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- W2077982059 title "Fresh and calcined supported 12-tungstosilicicacid: Synthesis, characterization and application to some acid catalyzed reactions" @default.
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- W2077982059 doi "https://doi.org/10.1016/j.molcata.2007.05.019" @default.
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