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• W2078019196 abstract "Two boron nitride (BN) nanostructures, the bamboo-like nanotubes and nanothorns where the nanosize h-BN layers are randomly stacked looking like thorns, were synthesized selectively via thermal chemical vapor deposition of B/B(2)O(3) under the NH(3) flow at 1200 degrees C. Electron energy-loss spectroscopy reveals the N-rich h-BN layers with a ratio of B/N = 0.75-0.85. Angle-resolved X-ray absorption near edge structure of these two N-rich nanostructures has been compared with that of h-BN microcrystals. The pi transition in the N K-edge shifts to the lower energy by 0.8-1.0 eV from that of h-BN microcrystals, and the second-order signals of N 1s electrons become significant. We suggest that the N enrichment would decrease the band gap of nanostructures from that of h-BN microcrystals. The Raman spectrum shows the peak broadening due to the defects of N-rich h-BN layers." @default.
• W2078019196 created "2016-06-24" @default.
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• W2078019196 date "2005-03-26" @default.
• W2078019196 modified "2023-10-01" @default.
• W2078019196 title "X-ray Absorption Near Edge Structure Study of BN Nanotubes and Nanothorns" @default.
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• W2078019196 doi "https://doi.org/10.1021/jp0464425" @default.
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