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- W2078020111 abstract "Salen-type bisoxime 5,5′-dimethoxy-2,2′-[(ethylenedioxy)bis(nitrilomethylidyne)]diphenol (H2L) and its trinuclear Ni(II) cluster {[(NiL)(n-BuOH)]2(μ-OAc)2Ni} · n-BuOH have been synthesized and structurally characterized. The structure of H2L adopts an L-shape conformation where the two salicylaldoxime moieties are well separated. In the trinuclear Ni(II) cluster, two acetates coordinate to three Ni(II)'s through Ni–O–C–O–Ni bridges, four μ-phenoxos from two [NiL(n-BuOH)] units also coordinate to Ni(II), and two n-butanols coordinate to two terminal Ni(II)'s forming a distorted octahedral geometry. The Ni–O–C–O–Ni and μ-phenoxo bridges play important roles in assembling Ni(II) and the ligands. H2L forms a rectangle-like large cave structure through O–H ··· N, C–H ··· O, and C–H ··· π hydrogen-bond interactions, whereas its trinuclear Ni(II) cluster exhibits a 3-D supramolecular network structure through intermolecular O–H ··· O, C–H ··· O, and C–H ··· π hydrogen-bond interactions." @default.
- W2078020111 created "2016-06-24" @default.
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- W2078020111 date "2012-05-29" @default.
- W2078020111 modified "2023-10-18" @default.
- W2078020111 title "A tetradentate bisoxime and its supramolecular nickel(II) cluster: synthesis, crystal structure, and spectral properties" @default.
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- W2078020111 doi "https://doi.org/10.1080/00958972.2012.693176" @default.
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