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• W2078096568 abstract "The volatile composition from four types of multifloral Portuguese (produced in Madeira Island) honeys was investigated by a suitable analytical procedure based on dynamic headspace solid-phase microextraction (HS-SPME) followed by thermal desorption gas chromatography-quadrupole mass spectrometry detection (GC-qMS). The performance of five commercially available SPME fibres: 100 microm polydimethylsiloxane, PDMS; 85 microm polyacrylate, PA; 50/30 microm divinylbenzene/carboxen on polydimethylsiloxane, DVB/CAR/PDMS (StableFlex); 75 microm carboxen/polydimethylsiloxane, CAR/PDMS, and 65 microm carbowax/divinylbenzene, CW/DVB; were evaluated and compared. The highest amounts of extract, in terms of the maximum signal obtained for the total volatile composition, were obtained with a DVB/CAR/PDMS coating fibre at 60 degrees C during an extraction time of 40 min with a constant stirring at 750 rpm, after saturating the sample with NaCl (30%). Using this methodology more than one hundred volatile compounds, belonging to different biosynthetic pathways were identified, including monoterpenols, C13-norisoprenoids, sesquiterpenes, higher alcohols, ethyl esters and fatty acids. The main components of the HS-SPME samples of honey were in average ethanol, hotrienol, benzeneacetaldehyde, furfural, trans-linalool oxide and 1,3-dihydroxy-2-propanone." @default.
• W2078096568 created "2016-06-24" @default.
• W2078096568 creator A5044834976 @default.
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• W2078096568 creator A5060924859 @default.
• W2078096568 date "2007-11-15" @default.
• W2078096568 modified "2023-10-11" @default.
• W2078096568 title "Screening of volatile composition from Portuguese multifloral honeys using headspace solid-phase microextraction-gas chromatography–quadrupole mass spectrometry" @default.
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• W2078096568 doi "https://doi.org/10.1016/j.talanta.2007.05.037" @default.
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