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- W2078133793 abstract "The facile synthesis of esters by lipase-catalysed esterification of fatty acids and ethanol is demonstrated. Evaporation of the water generated in the reaction allowed the rapid production of esters of >99% yield in refluxing pentane or hexane. Water was trapped by condensing the refluxing vapor phase and passing it over activated molecular sieves in a reflux trap. High yields were rapidly obtained in synthesis of ethyl esters of oleic, linoleic, α-linolenic, and arachidonic acids without peroxidation of double bonds. The wax ester oleyl oleate was also synthesized rapidly with little peroxidation. A molar excess of 1.25 to 1.5 of ethanol allowed the most rapid ester synthesis. Synthesis of ethyl stearate was carried out on a preparative scale (50 g). Greater than 99% conversion was obtained in 50 min." @default.
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- W2078133793 date "1992-07-01" @default.
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- W2078133793 title "Facile synthesis of fatty acid esters in high yields" @default.
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- W2078133793 doi "https://doi.org/10.1016/0141-0229(92)90125-8" @default.
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