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- W2078148933 abstract "Quadrupolar nuclei yield Fourier transform magic-angle spinning NMR spectra exhibiting many spinning sidebands. The widths and the intensities of the sidebands are very sensitive functions of the angle the spinning axis makes with the magnetic field. This dependence can be used in adjusting the spinning angle at least to within ± 0.1° of the magic angle. In particular, the 79Br signal from powdered KBr is especially convenient for monitoring the angle in 13C MAS experiments. Large (approximately 3 mm) crystals of KBr offer greater sensitivity to angle, but are less convenient to use than powder. NaBr, KBrO3, and K55MnO4 were also tested and found to be less suitable as angle markers than is KBr." @default.
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- W2078148933 date "1982-06-01" @default.
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- W2078148933 title "Setting the magic angle using a quadrupolar nuclide" @default.
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- W2078148933 doi "https://doi.org/10.1016/0022-2364(82)90243-8" @default.
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