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- W2078150537 abstract "Abstract The synthesis and characterization of organometallic and inorganic cobalt(III) compounds of the type trans-[Co(dpgH)2(R)(L)] are reported, where dpgH represents diphenylglyoximate monoanion, R = Cl, CH3, CH2CH3, CH2CI or iBu; and L is either an organic N-donor ligand (pyridine, 3,5-lutidine or γ-picoline), or trimethylphosphite. Their structural and spectroscopic properties are studied and compared with those previously reported for analogous compounds containing dimethylglioximato(−1), (dmgH); glyoximato(−1), (gH), or N2,N2′-propanediylbis(2,3-butanedione, 2-imine-3-oxime), ((DO)(DOH)pn), as equatorial ligands. The 1H-NMR chemical shifts of the axial R group in the diphenylglyoximato compounds can be accurately estimated from those of the dimethylglyoximato or glyoximato analogues and allow the detectin of electronic cis-effects. The first X-ray crystal structure of an organometallic bis(diphenylglyoximato)(cobalt(III) compound, [Co(dpgH)2(CH3)(py)], is reported. The CoC bond length in this type of complex seems not to be sensitive to changes in equatorial ligands." @default.
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- W2078150537 date "1991-08-01" @default.
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- W2078150537 title "New organometallic cobaloximes containing an equatorial diphenylglyoximato(−1) ligand. Comparison between their properties and those of other B12 model compounds. Crystal structure of trans-[Co(dpgH)2(CH3)(pyridine)]" @default.
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- W2078150537 doi "https://doi.org/10.1016/0022-328x(91)86105-y" @default.
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