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• W2078234286 abstract "We report herein the syntheses of dodecamethoxytricyclobutabenzene (TCBB) 1 and hexaoxo-TCBB 2, a class of molecules with structural and theoretical interest. The preparation is based on the 3-fold [2 + 2] cycloadditions of benzyne and ketene silyl acetals (KSAs), where the selectively protected 2-iodophloroglucinol derivative served as a synthetic equivalent of benztriyne I, allowing rapid and regioselective annulation of fully functionalized four-membered rings. Structural study on the former compound showed that the C−C bond lengths in the central benzene ring were essentially the same." @default.
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• W2078234286 date "2006-07-15" @default.
• W2078234286 modified "2023-10-18" @default.
• W2078234286 title "Dodecamethoxy- and Hexaoxotricyclobutabenzene: Synthesis and Characterization" @default.
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• W2078234286 doi "https://doi.org/10.1021/ja064063e" @default.
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