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- W2078260079 abstract "We present a facile, high-yield synthetic route to linear poly(dibutylstannane) of relatively high molecular weight (Mw = 20 × 103 g mol−1) through dehydropolymerization of dibutylstannane with the catalyst [RhCl(PPh3)3]. Unlike previously synthesized polystannanes, the present materials were entirely free of cyclic oligomers. A reversible phase transition was observed at a temperature of ∼1 °C, which was found to be associated with a marked change in crystalline order. The material appeared to be in a liquid-crystalline-like state at room temperature and could be readily oriented by simple shearing processes, which resulted in highly ordered films." @default.
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- W2078260079 date "2005-01-01" @default.
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- W2078260079 title "Facile synthesis of linear poly(dibutylstannane)" @default.
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