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- W2078277514 abstract "A novel chemical alloying method has been developed for the fabrication of nanocrystalline thermoelectric alloy Bismuth telluride, Bi2Te3. The method consists of a combination of solution chemical method and thermal processing under controlled heating conditions. The components have been coprecipitated from a solution and the precursor consists of a solid solution of the different intermediate compounds and exhibits high reactivity. Calcination and hydrogen reduction of the precursor at moderate temperature, 350 °C, for 2 h resulted in the alloying of these elements to obtain the pure phase of the thermoelectric material in fine powder. The method is simpler than conventional melt processing and produced a 95–98% yield in laboratory scale. High concentration of grain boundaries provided by nanostructuring is expected to lower the thermal conductivity of thermoelectric material and further increase the performance." @default.
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- W2078277514 date "2003-08-01" @default.
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- W2078277514 title "Chemical alloying and characterization of nanocrystalline bismuth telluride" @default.
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- W2078277514 doi "https://doi.org/10.1016/s0167-577x(03)00250-7" @default.
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