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- W2078311087 abstract "A synthesis of 2-substituted-1,3-dienes is reported which uses silicon as a control element: Eight aldehydes were converted into α-silyl ketones by treatment with trimethylsilylmethylmagnesium chloride and rapid Collins oxidation. Addition of vinylmagnesium bromide to the resulting α-silyl ketones, followed by Peterson elimination, gave a series of dienes. The route was used to make (4S)-3-methylene-t-[(phenylmethoxy)methoxy]pent-1-ene from (–)-ethyl lactate; low asymmetric induction was observed in the Diels–Alder reactions of this diene with diethyl fumarate and N-phenylmaleimide." @default.
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- W2078311087 date "2010-08-22" @default.
- W2078311087 modified "2023-09-26" @default.
- W2078311087 title "ChemInform Abstract: Silicon-Directed Diene Synthesis." @default.
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- W2078311087 doi "https://doi.org/10.1002/chin.199146108" @default.
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