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• W2078330774 startingPage "7996" @default.
• W2078330774 abstract "Abstract A modified Julia–Kocienski protocol was investigated for the synthesis of CF 3 ‐substituted terminal olefins. By employing a simple one‐step procedure, aldehydes were converted into the corresponding CF 3 ‐substituted olefins using 2‐[(2,2,2‐trifluoroethyl)sulfonyl]benzo[ d ]thiazole as the trifluoromethylation agent. This sulfone was prepared on a gram scale in two steps from inexpensive and commercially available trifluoroethanol. The Julia–Kocienski olefination tolerated various functional groups, and the trifluoromethylated olefins were obtained in good yields. However, the E / Z selectivity was strongly substrate dependent, and only moderate selectivities could be achieved." @default.
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• W2078330774 date "2013-10-09" @default.
• W2078330774 modified "2023-10-10" @default.
• W2078330774 title "Synthesis of CF₃-Substituted Olefins by Julia-Kocienski Olefination Using 2-[(2,2,2-Trifluoroethyl)sulfonyl]benzo[<i>d</i>]thiazole as Trifluoromethylation Agent" @default.
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• W2078330774 doi "https://doi.org/10.1002/ejoc.201301070" @default.
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