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- W2078393048 abstract "Abstract 5-allyl-2-hydroxy-3-methoxyazobenzene was preperad by the reaction of 4-allyl-2-methoxyfenol and benzenediazoniumchloride and crystallized from dimethylsulphoxide to yield crystals suitable for analysis. The molecular structure was identified by UV-VIS, IR, 1H-NMR, 13C-NMR and elemental analysis. The crystal structure of the title compound was determined as monoclinic by by single crystal X-Ray diffraction technique. The crystal parameters of this compound are as follows: monoclinic P 2 1/n, a=5.559(2) A,b=14.900(2) A, c= 17.573(29 A, P = 98.58(1)†, V = 1439.3(2) A3, Z = 2, Dx = 0.610 g/cm3, F(OOO) = 284, λ (MoKα) = 0.71070 A, μ = 0.041 mm−1. The structure was solved by SHELXS-86 and refined by SHELXL-93. R = 0.09 for 1107 observed reflections with I > 2σ (I)." @default.
- W2078393048 created "2016-06-24" @default.
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- W2078393048 date "1997-12-01" @default.
- W2078393048 modified "2023-10-18" @default.
- W2078393048 title "Structure of 5-Allyl-2-hydroxy-3-methoxyazobenzene" @default.
- W2078393048 doi "https://doi.org/10.1080/00387019708006742" @default.
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