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- W2078442929 abstract "An improved gas chromatographic method is described for the determination of alkyl- and alkoxy-substituted phenols as their 2,4-dinitrophenyl ethers. The gas chromatographic analysis is performed on OV-210 glass capillary or SP-2100 fused silica capillary columns using electron-capture detection. The separation of o-, m- and p-substituted phenols and the isomers of dimethylphenols has been achieved. The sensitivity limit of electron-capture detection for various, 2,4-dinitrophenyl ethers is 0.01–0.09 ng injected and the coefficient of variation is about 5%. The reaction conditions for ether formation are described. The optimum pH, temperature and reaction time are 11.5, 50°C and 40 min, respectively." @default.
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- W2078442929 date "1980-12-01" @default.
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- W2078442929 title "Gas chromatographic determination of phenols as 2,4-dinitrophenyl ethers using glass capillary columns and an electron-capture detector" @default.
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- W2078442929 doi "https://doi.org/10.1016/s0021-9673(00)91826-0" @default.
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