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- W2078459839 abstract "A simple and precise high-performance liquid chromatographic (HPLC) procedure was developed for the determination of cefsulodin, a new antipseudomonal cephalosporin antibiotic, in plasma. The analytical procedure involved ultrafiltration of samples that were buffered to prevent cefsulodin degradation, followed by injection into an HPLC system, utilizing a C18 reversed-phase analytical column, a mobile phase of acetonitrile-modified aqueous acetate buffer, and a UV spec-trophotometric detector. Because of the simplicity of the procedure, the intraassay (~2%) and interassay (~3-4%) coefficients of variation were extremely low. Recoveries of drug were essentially quantitative in freshly buffered specimens and in those stored buffered and frozen for nearly 3 months. Calibration curves were rectilinear from the limit of quantification (~0.2 μg/ml) to 200 fig/ml, as demonstrated by regression correlation coefficients averaging >0.999 during routine analyses." @default.
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- W2078459839 date "1982-10-01" @default.
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- W2078459839 title "Precise High-Performance Liquid Chromatographic Procedure for the Determination of Cefsulodin, a New Antipseudomonal Cephalosporin Antibiotic, in Plasma" @default.
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- W2078459839 doi "https://doi.org/10.1002/jps.2600711008" @default.
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