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• W2078543913 abstract "The crystal structure of bulk microcrystalline material obtained by interaction of two rigid building blocks, namely dirhodium(II) tetra(trifluoroacetate), [Rh2(O2CCF3)4], and bis(4’-pyridyl)diphenylsilane, (C6H5)2Si(C5H4N)2, has been solved ab initio using X-ray powder diffraction data. The title product of the 1 ∶ 1 composition, [Rh2(O2CCF3)4·(µ2-(C6H5)2Si(C5H4N)2)], is a one-dimensional zigzag polymer built on axial Rh⋯N interactions averaged at 2.16 Å. Its structural characterization complements the previously reported product of the 2 ∶ 1 composition obtained from the same reaction, namely {[Rh2(O2CCF3)4]2·(µ4-(C6H5)2Si(C5H4N)2)}. The latter has a 2D layered network revealed by the single crystal diffraction study. A combination of powder and single crystal X-ray techniques is shown to be methodologically important and complementary for understanding of product assembling in the system." @default.
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• W2078543913 date "2004-01-01" @default.
• W2078543913 modified "2023-09-23" @default.
• W2078543913 title "Bulk material vs. single crystal: powder diffraction to the rescue" @default.
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• W2078543913 doi "https://doi.org/10.1039/b412701n" @default.
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