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- W2078570504 abstract "The title compound exhibits a transition at about 745 K detectable by DSC and dielectric measurements. The structure was determined at ambient temperature and above the transition. In both cases, the cell is orthorhombic with a = 13.139(4), b = 10.413(6), c = 9.239(6)Å at 295 K and a = 13.302(4), b = 10.506(7), c = 9.240(5) Å at 795 K, Z = 4. The structures were refined in space group Pnma to R values of 0.048 and 0.058 using 1472 and 1154 unique single-crystal reflections, respectively. The two structures are very similar and can be described as a three-dimensional network of distorted BiO6 octahedra and PO4 tetrahedra. At high temperature, one of the PO4 tetrahedra is statistically disordered over two positions related by the mirror. Below the transition temperature, ordering of this ion leads to doubling of the c parameter and formation of satellite reflections (h, k, l + 12). Extinction rules indicate P21ca as a possible supercell space group." @default.
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- W2078570504 date "1986-05-01" @default.
- W2078570504 modified "2023-10-18" @default.
- W2078570504 title "The crystal structure, phase transition, and dielectric properties of K2Bi3(PO4)3O, a new oxyphosphate" @default.
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- W2078570504 doi "https://doi.org/10.1016/0022-4596(86)90250-1" @default.
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