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- W2078606327 abstract "Abstract Eledoisin is a peptide with complex pharmacological properties and recognized therapeutical application. Peptides of pharmaceutical interest in the molecular mass range of eledoisin are often synthesized using solid-phase peptide synthesis. This procedure results in complex crudes of reaction that require extensive purification and characterization. In order to avoid long empirical optimization procedures to separate the unwanted products associated with the target peptide eledoisin from a synthesis crude, the method of linear solvation energy relationships for predicting peptide retention times was applied and the proportion of the organic modifier of the mobile phase used in high-performance liquid chromatography (HPLC) method was optimized. The crude of synthesis was also analyzed by combined HPLC–electrospray ionization mass spectrometry, which allowed rapid and reliable identification of the target peptide and has furnished comprehensive information on other reaction products." @default.
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- W2078606327 date "1999-06-01" @default.
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- W2078606327 title "Fractionation and characterization of a crude peptide mixture from the synthesis of eledoisin by liquid chromatography–electrospray ionization mass spectrometry" @default.
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- W2078606327 doi "https://doi.org/10.1016/s0021-9673(99)00294-0" @default.
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