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• W2078655084 abstract "One-step synthesis of block-graft copolymers by reversible addition-fragmentation chain transfer (RAFT) and ring-opening polymerization (ROP) by using a novel initiator was reported. Block-graft copolymers were synthesized in one-step by simultaneous RAFT polymerization of n-butylmethacrylate (nBMA) and ROP of e-caprolacton (CL) in the presence of a novel macroinitiator (RAFT-ROP agent). For this purpose, first epichlorohydrin (EPCH) was polymerized by using H2SO4 via cationic ring-opening mechanism. And then a novel RAFT-ROP agent was synthesized by the reaction of potassium ethyl xanthogenate and polyepichlorohydrin (poly-EPCH). By using the RAFT-ROP agent, poly[CL-b-EPCH-b-CL-(g-nBMA)] block-graft copolymers were synthesized. The principal parameters such as monomer concentration, initiator concentration, and polymerization time that affect the one-step polymerization reaction were evaluated. The block lengths of the block-graft copolymers were calculated by using 1H-nuclear magnetic resonance (1H NMR) spectrum. The block length could be adjusted by varying the monomer and initiator concentrations. The characterization of the products was achieved using 1H NMR, Fourier-transform infrared spectroscopy, gel-permeation chromatography, thermogravimetric analysis, differential scanning calorimetry, elemental analysis, and fractional precipitation (γ) techniques. © 2013 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2013, 51, 2651–2659" @default.
• W2078655084 created "2016-06-24" @default.
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• W2078655084 date "2013-03-26" @default.
• W2078655084 modified "2023-10-11" @default.
• W2078655084 title "One-step synthesis of block-graft copolymers via simultaneous reversible-addition fragmentation chain transfer and ring-opening polymerization using a novel macroinitiator" @default.
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• W2078655084 doi "https://doi.org/10.1002/pola.26654" @default.
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