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- W2078691129 abstract "Self assembly monolayers of octadecyltrichlorosilane Cl3–Si–(CH2)17–CH3 and 17-cyanoheptadecyltrichlorosilane (CTS) Cl3–Si–(CH2)17–CN on silicon wafers have been prepared by adsorption from solution. The molecular orientation within the monolayers was investigated by using polarisation modulation FTIR spectroscopy. Quantitative analysis reveals that both types of silanes — monofunctionalised and bifunctionalised — form highly ordered monolayers when prepared from solutions. Weak CH2 stretching modes indicate a high degree of order as well as a small tilt angle of the molecular backbone with respect to the surface normal. The decomposition of the terminal nitrile group of the substituted silane into a carboxyl group could be identified. The decomposition is caused by a high HCl concentration, which develops upon binding of 17-CTS to the OH groups of the silicon surface." @default.
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- W2078691129 date "2001-05-01" @default.
- W2078691129 modified "2023-10-03" @default.
- W2078691129 title "Characterisation of ultra-thin polymer films by polarisation modulation FTIR spectroscopy" @default.
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- W2078691129 doi "https://doi.org/10.1016/s0022-2860(01)00438-0" @default.
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