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- W2078737886 abstract "Summary An improved method for preparing β-lactose crystals was developed by heating a supersaturated solution of lactose under reflux. The product obtained by this method yielded large well-defined crystals. Differential thermal analysis was used for the characterization of β-lactose. The thermograms of β-lactose obtained when heating conditions were similar to those used in the conventional measurement of the melting point gave an endothermic peak at 229·5–230 °C. A marked difference was observed between the peak temperature on the thermogram and the melting point (m.p.) of β-lactose (252–252·2 °C) given in the literature. The method for determining the m.p. of β-lactose was reexamined in detail and previously reported values could not be confirmed. By application of the conventional method for determining m.p. of organic substances, 229·5 °C (dec.) is proposed as the m.p. of β-lactose." @default.
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- W2078737886 date "1978-10-01" @default.
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- W2078737886 title "An improved method for the preparation of crystalline β-lactose and observations on the melting point" @default.
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- W2078737886 doi "https://doi.org/10.1017/s0022029900016587" @default.
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