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- W2078781179 abstract "Abstract The structure of the orthorhombic room-temperature phase of Cu 8 GeS 6 (phase II) has been refined successfully on the basis of X-ray diffraction data from a 12-fold twinned crystal. The symmetry operations and the unit cell of the pseudo-cubic expression are (0,0,0; 1/2,1/2,0)+ x , y , z ; y , x , z ; 1/4− x ,3/4− y ,1/2+ z ; 3/4− y ,1/4− x ,1/2+ z ; a = b =9.907 A, c =9.870 A, α = β =90°, γ =90.64°, whose standard settings are Pmn2 1 ; A =7.045, B =6.966, C =9.870 A. Among the twin domains 1–6, the argyrodite-type GeS 6 frameworks can be superposed to each other in principle, and only Cu–Cu network directions differ. The minor twin domains 7–12 are respectively related to the major domains 1–6 by a two-fold rotation on [111]. In the high-temperature phase (phase I) of Cu 8 GeS 6 , Cu ions are expected to distribute statistically over many sites in the framework. On cooling through the phase-transition temperature, the crystal can be converted into a multiple twin of phase II. Cu ions are transferred to five kinds of independent sites from the statistical distribution state." @default.
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- W2078781179 date "2000-11-02" @default.
- W2078781179 modified "2023-09-27" @default.
- W2078781179 title "Multiple-twinned crystal of the room-temperature phase of Cu8GeS6" @default.
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- W2078781179 doi "https://doi.org/10.1016/s0167-2738(00)00494-x" @default.
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