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- W2078858634 abstract "Die Verbindungen ASbO2 (A = K/Rb; monoklin, C2/c, a = 785.4(3)/799.6(1) pm, b = 822.1(4)/886.32(7) pm, c = 558.7(3)/559.32(5) pm, β = 124.9(1)/123.37(6)°, Z = 4) sind isotyp zu CsSbO2 und den korrespondierenden Bismutaten. Die Strukturen der Antimonate A4Sb2O5 (A = K/Rb: orthorhombisch, Cmcm, a = 394.9(1)/407.34(7) pm, b = 1807.4(1)/1893.5(1) pm, c = 636.34(9)/655.60(8) pm, Z = 2) und Cs4Sb2O5 (monoklin, Cm, a = 1059.81(7) pm, b = 692.68(8) pm, c = 811.5(1) pm, β = 98.7(1)°, Z = 2) enthalten isolierte Anionen [O2SbOSbO2]4–. Cs3SbO4 (orthorhombisch, Pnma, a = 1296.1(1) pm, b = 919.24(8) pm, c = 679.95(6) pm, Z = 4) ist isotyp zu K3NO4. Alkaline Metal Oxoantimonates: Synthesis, Crystal Structures, and Vibrational Spectroscopy of ASbO2 (A = K, Rb), A4Sb2O5 (A = K, Rb, Cs), and Cs3SbO4 The compounds ASbO2 (A = K/Rb; monoclinic, C2/c, a = 785.4(3)/799.6(1) pm, b = 822.1(4)/886.32(7) pm, c = 558.7(3)/559.32(5) pm, β = 124.9(1)/123.37(6)°, Z = 4) are isotypic with CsSbO2 and the corresponding bismutates. The structures of the antimonates A4Sb2O5 (A = K/Rb: orthorhombic, Cmcm, a = 394.9(1)/407.34(7) pm, b = 1807.4(1)/1893.5(1) pm, c = 636.34(9)/655.60(8) pm, Z = 2) and Cs4Sb2O5 (monoclinic, Cm, a = 1059.81(7) pm, b = 692.68(8) pm, c = 811.5(1) pm, β = 98.7(1)°, Z = 2) both contain the anion [O2SbOSbO2]4–. Cs3SbO4 (orthorhombic, Pnma, a = 1296.1(1) pm, b = 919.24(8) pm, c = 679.95(6) pm, Z = 4) crystallizes with the K3NO4 structure type." @default.
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- W2078858634 date "2000-06-01" @default.
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- W2078858634 title "Alkalimetall-Oxoantimonate: Synthesen, Kristallstrukturen und Schwingungsspektren von ASbO2 (A = K, Rb), A4Sb2O5 (A = K, Rb, Cs) und Cs3SbO4" @default.
- W2078858634 doi "https://doi.org/10.1002/(sici)1521-3749(200006)626:6<1305::aid-zaac1305>3.0.co;2-l" @default.
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