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- W2078889675 abstract "[Fe2(μ-CO)(CO)6(μ-H)(μ-PBut2)] (2) has been synthesized from Na[Fe2(μ-CO)(CO)6(μ-PBut2)] and CH3COOH and structurally characterized by X-ray analysis. Also the crystal structure of PPN[Fe2(μ-CO)(CO)6(μ-PBut2)] (1) containing the parent complex anion to 2 has been determined. The two structures were refined to conventional R values of 0.034 and 0.021 for 5481 and 2825 observed reflections, respectively. Structural comparisons of 1 and Et4N[Fe2(μ-CO)(CO)6(μ-PPh2)] (4) as well as of 1, 2 and the isolobal cluster compounds to 2, [Fe2[μ-Ag(PPh3)] (μ-CO)(CO)6(μ-PBut2)] (3) and [Fe2[μ-Cu(PPh3)] (μ-CO)(CO)6(μ-PPh2)] (5) are made. Unexpectedly the FeFe bond in 2 is significantly shorter than in the deprotonated parent anion of 1." @default.
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- W2078889675 date "1994-10-01" @default.
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- W2078889675 title "X-ray crystal structures of PPN[Fe2(μ-CO)(CO)6(μ-PBu′2)] [PPN = (PPh3)2N+] and [Fe2(μ-CO)(CO)6(μ-H)(μ-PBut2)] and structural comparison with the cluster [Fe2[μ-Ag(PPh3)](μ-CO)(CO)6(μ-PBut2)]" @default.
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- W2078889675 doi "https://doi.org/10.1016/s0277-5387(00)86622-x" @default.
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