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- W2078964945 abstract "Para-disubstituted benzene molecules (p-xylene, p-chlorotoluene, p-dichlorobenzene and p-dibromobenzene) have been sorbed in an MFI type zeolitic material presenting the H0.60Al0.60Si95.40O192 framework composition. At room temperature, the evacuated form of this highly siliceous ZSM-5 phase presents the monoclinic symmetry. At lower sorbate-loadings (n = 2–3 moleculesunit-cell) the four MFI·nsorbate complexes crystallize in the orthorhombic Pnma space group. X-ray powder profile refinements and energy-minimization simulations show that the sorbate molecules are located at the channel-intersections (sites I). The individual molecules interact near sites III (through the straight-channels) and form dimeric molecular associations. These dimers are oriented parallel to the b-axis direction and are statistically distributed in the crystal structure. At n = 4, the associated molecules form infinite polymeric chains in the 010 direction. The atomic positions of the topology and of the guest molecules have been refined by using linear constraints." @default.
- W2078964945 created "2016-06-24" @default.
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- W2078964945 date "1992-08-01" @default.
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- W2078964945 title "Characterization of guest molecules sorbed in zeolites of known structure. Part IV — Localization of para-disubstituted benzene molecules at low sorbate-fillings in a zsm-5 material ()" @default.
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- W2078964945 doi "https://doi.org/10.1016/0025-5408(92)90195-6" @default.
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