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- W2079058942 abstract "Treatment of 1-Boc-1-tosyl-hydrazine with 1,1,3,3-tetramethylguanidine (TMG) gave rise to two products, one containing and the other not containing TMG. The latter was identified as 1-Boc-2-tosyl-hydrazine. This rearrangement provided useful insight into the nature of the first product that had previously been isolated and assigned an incorrect tentative structure. To rationalize the results a plausible mechanism via a common intermediate, involving TMG as a nucleophilic catalyst is proposed. A simpler procedure for the preparation of the starting material is also presented." @default.
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- W2079058942 date "2014-12-01" @default.
- W2079058942 modified "2023-10-17" @default.
- W2079058942 title "An unprecedented rearrangement of a 1,1-diprotected hydrazine derivative. Structure revision of a catalyst-containing by-product" @default.
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- W2079058942 doi "https://doi.org/10.1016/j.tetlet.2014.10.121" @default.
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