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• W2079080785 abstract "To obtain direct evidence of the formation of the Ni-Mo-S phase on NiMo/Al(2)O(3) catalysts under high-pressure hydrodesulfurization conditions, a high-pressure EXAFS chamber has been constructed and used to investigate the coordination structure of Ni and Mo species on the catalysts sulfided at high pressure. The high-pressure chamber was designed to have a low dead volume and was equipped with polybenzimidazole X-ray windows. Ni K-edge k(3)chi(k) spectra with high signal-to-noise ratio were obtained using this high-pressure chamber for the NiMo/Al(2)O(3) catalyst sulfided at 613 K and 1.1 MPa over a wide k range (39.5-146 nm(-1)). The formation of Ni-Mo and Mo-Ni coordination shells was successfully proved by Ni and Mo K-edge EXAFS measurement using this chamber. Interatomic distances of these coordination shells were almost identical to those calculated from Ni K-edge EXAFS of NiMo/C catalysts sulfided at atmospheric pressure. These results support the hypothesis that the Ni-Mo-S phase is formed on the Al(2)O(3)-supported NiMo catalyst sulfided under high-pressure hydrodesulfurization conditions." @default.
• W2079080785 created "2016-06-24" @default.
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• W2079080785 date "2010-03-19" @default.
• W2079080785 modified "2023-10-16" @default.
• W2079080785 title "<i>In situ</i>observation of Ni–Mo–S phase formed on NiMo/Al₂O₃catalyst sulfided at high pressure by means of Ni and Mo<i>K</i>-edge EXAFS spectroscopy" @default.
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• W2079080785 doi "https://doi.org/10.1107/s0909049510004802" @default.
• W2079080785 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20400842" @default.
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