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- W2079116738 abstract "In this paper, we describe some observations from the attempted reaction of Br - BsubPc with phenol in DMF and DMAc. During these efforts, we found that Br - BsubPc reacts with the respective solvents to produce axially substituted formate- BsubPc and acetate- BsubPc . When no phenol is present the reaction proceeds to completion in a relatively short period of time. However, when phenol was present in DMF the reaction produced a mixture of formate- BsubPc , phenoxy- BsubPc , and HO - BsubPc . Similar results were found for the less-reactive Cl - BsubPc and MsO - BsubPc . Aside from these observations, it was found that simple heating in wet acetone of Br - BsubPc quantitatively produced HO - BsubPc after a facile workup. This method of producing HO - BsubPc removes the high temperatures, long reaction times, and harmful chemicals required in other synthetic methods. These results are relevant to anyone considering the reaction of BsubPcs in polar aprotic solvents." @default.
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- W2079116738 date "2014-10-01" @default.
- W2079116738 modified "2023-10-14" @default.
- W2079116738 title "Some observations regarding the behavior of boron subphthalocyanines in polar aprotic solvents" @default.
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- W2079116738 doi "https://doi.org/10.1142/s1088424614500886" @default.
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