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- W2079147181 abstract "Silica gel samples, modified with 3-aminopropyltriethoxy silane (APTS), have been prepared by sequentially sampling the substrate from the reaction vessel at various time intervals, and the Raman spectra of these samples have been measured. The CH stretch Raman bands at 2938 and 2981 cm−1 became more intense as the reaction proceeded. Kinetic analyses were then carried out, after making the assumption that the time dependence of relative Raman peak heights (I2938/I800 and I2981/I800) is a pseudo-first order. The rate constants obtained are k=8.05×10−4 s−1 for the 2938 cm−1 band and k=9.45×10−4 s−1 for the 2981 cm−1 band. We may assume that the dependence of the change in intensity of the CH stretch Raman bands on time is a reflection of the change in conformation of the APS moieties." @default.
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- W2079147181 date "1997-03-01" @default.
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- W2079147181 title "Raman scattering study of the interaction of 3-aminopropyltriethoxy silane on silica gel. Time-dependent conformational change of aminopropylsilyl segments" @default.
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- W2079147181 doi "https://doi.org/10.1016/s0924-2031(96)00069-0" @default.
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