FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2079154608> ?p ?o ?g. }

• W2079154608 endingPage "36" @default.
• W2079154608 startingPage "28" @default.
• W2079154608 abstract "An ultra-performance liquid chromatography tandem mass spectrometry (UPLC™–MS/MS) assay was developed for the simultaneous analysis of histamine, its major metabolite tele-methylhistamine, and an internal standard (N-tele-(R)-α-dimethylhistamine) from human cerebrospinal fluid (CSF) samples. The method involves derivatization of primary amines with 4-bromobenzenesulfonyl chloride and subsequent analysis by reversed phase liquid chromatography with mass spectrometry detection and positive electrospray ionization. The separation of derivatized biogenic amines was achieved within 3.5 min on an Acquity® BEH C18 column by elution with a linear gradient of acetonitrile/water/formic acid (0.1%). The assay was linear in the concentration range of 50–5000 pM for each amine (5.5–555 pg/ml for histamine and 6.25–625 pg/ml for tele-methylhistamine). For repeatability and precision determination, coefficients of variation (CVs) were less than 11.0% over the tested concentration ranges, within acceptance criteria. Thus, the developed method provides the rapid, easy, highly sensitive, and selective requirement to quantify these amines in human CSF. No significant difference was found in the mean ± standard error levels of these amines between a group of narcoleptic patients (histamine = 392 ± 64 pM, tele-methylhistamine = 2431 ± 461 pM, n = 7) and of neurological control subjects (histamine = 402 ± 72 pM, tele-methylhistamine = 2209 ± 463 pM, n = 32)." @default.
• W2079154608 created "2016-06-24" @default.
• W2079154608 creator A5010298377 @default.
• W2079154608 creator A5021696638 @default.
• W2079154608 creator A5022326769 @default.
• W2079154608 creator A5070569366 @default.
• W2079154608 creator A5071168732 @default.
• W2079154608 creator A5088488166 @default.
• W2079154608 date "2011-02-01" @default.
• W2079154608 modified "2023-10-17" @default.
• W2079154608 title "Histamine and tele-methylhistamine quantification in cerebrospinal fluid from narcoleptic subjects by liquid chromatography tandem mass spectrometry with precolumn derivatization" @default.
• W2079154608 cites W1493410983 @default.
• W2079154608 cites W1533063439 @default.
• W2079154608 cites W1967884630 @default.
• W2079154608 cites W2002299903 @default.
• W2079154608 cites W2013146593 @default.
• W2079154608 cites W2027131886 @default.
• W2079154608 cites W2027906637 @default.
• W2079154608 cites W2028268849 @default.
• W2079154608 cites W2033950872 @default.
• W2079154608 cites W2041652835 @default.
• W2079154608 cites W2044974821 @default.
• W2079154608 cites W2047295742 @default.
• W2079154608 cites W2052755701 @default.
• W2079154608 cites W2061409645 @default.
• W2079154608 cites W2069163972 @default.
• W2079154608 cites W2074292769 @default.
• W2079154608 cites W2079455913 @default.
• W2079154608 cites W2087404913 @default.
• W2079154608 cites W2121795503 @default.
• W2079154608 cites W2123035658 @default.
• W2079154608 cites W2139470111 @default.
• W2079154608 cites W2140347699 @default.
• W2079154608 doi "https://doi.org/10.1016/j.ab.2010.09.045" @default.
• W2079154608 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20932951" @default.
• W2079154608 hasPublicationYear "2011" @default.
• W2079154608 type Work @default.
• W2079154608 sameAs 2079154608 @default.
• W2079154608 citedByCount "39" @default.
• W2079154608 countsByYear W20791546082012 @default.
• W2079154608 countsByYear W20791546082013 @default.
• W2079154608 countsByYear W20791546082014 @default.
• W2079154608 countsByYear W20791546082015 @default.
• W2079154608 countsByYear W20791546082016 @default.
• W2079154608 countsByYear W20791546082017 @default.
• W2079154608 countsByYear W20791546082018 @default.
• W2079154608 countsByYear W20791546082019 @default.
• W2079154608 countsByYear W20791546082020 @default.
• W2079154608 countsByYear W20791546082021 @default.
• W2079154608 countsByYear W20791546082022 @default.
• W2079154608 crossrefType "journal-article" @default.
• W2079154608 hasAuthorship W2079154608A5010298377 @default.
• W2079154608 hasAuthorship W2079154608A5021696638 @default.
• W2079154608 hasAuthorship W2079154608A5022326769 @default.
• W2079154608 hasAuthorship W2079154608A5070569366 @default.
• W2079154608 hasAuthorship W2079154608A5071168732 @default.
• W2079154608 hasAuthorship W2079154608A5088488166 @default.
• W2079154608 hasConcept C1122143 @default.
• W2079154608 hasConcept C126322002 @default.
• W2079154608 hasConcept C154020017 @default.
• W2079154608 hasConcept C162356407 @default.
• W2079154608 hasConcept C179998833 @default.
• W2079154608 hasConcept C185592680 @default.
• W2079154608 hasConcept C2776923573 @default.
• W2079154608 hasConcept C2777379063 @default.
• W2079154608 hasConcept C2780626841 @default.
• W2079154608 hasConcept C31827203 @default.
• W2079154608 hasConcept C40684141 @default.
• W2079154608 hasConcept C43617362 @default.
• W2079154608 hasConcept C64489805 @default.
• W2079154608 hasConcept C71043704 @default.
• W2079154608 hasConcept C71924100 @default.
• W2079154608 hasConceptScore W2079154608C1122143 @default.
• W2079154608 hasConceptScore W2079154608C126322002 @default.
• W2079154608 hasConceptScore W2079154608C154020017 @default.
• W2079154608 hasConceptScore W2079154608C162356407 @default.
• W2079154608 hasConceptScore W2079154608C179998833 @default.
• W2079154608 hasConceptScore W2079154608C185592680 @default.
• W2079154608 hasConceptScore W2079154608C2776923573 @default.
• W2079154608 hasConceptScore W2079154608C2777379063 @default.
• W2079154608 hasConceptScore W2079154608C2780626841 @default.
• W2079154608 hasConceptScore W2079154608C31827203 @default.
• W2079154608 hasConceptScore W2079154608C40684141 @default.
• W2079154608 hasConceptScore W2079154608C43617362 @default.
• W2079154608 hasConceptScore W2079154608C64489805 @default.
• W2079154608 hasConceptScore W2079154608C71043704 @default.
• W2079154608 hasConceptScore W2079154608C71924100 @default.
• W2079154608 hasIssue "1" @default.
• W2079154608 hasLocation W20791546081 @default.
• W2079154608 hasLocation W20791546082 @default.
• W2079154608 hasOpenAccess W2079154608 @default.
• W2079154608 hasPrimaryLocation W20791546081 @default.
• W2079154608 hasRelatedWork W2081478254 @default.
• W2079154608 hasRelatedWork W2168408094 @default.
• W2079154608 hasRelatedWork W2317943501 @default.
• W2079154608 hasRelatedWork W2606142292 @default.
• W2079154608 hasRelatedWork W2806647571 @default.
• W2079154608 hasRelatedWork W2899901573 @default.

• next