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- W2079160699 abstract "Titanocene, zirconocene, and hafnocene dichlorides were reduced in the presence of terminally disubstituted 1,6-heptadiyne or 1,7-octadiyne to produce dicyclopentadienylmetallabicyclooctadienes and -nonadienes. The compounds were characterized by elemental analysis and 1H and 13C NMR spectrometry, and (C5H5)2HfC7H6[Si(CH3)3]2 was characterized by X-ray diffraction techniques. The compounds crystallized in the triclinic space group P1 in a unit cell of dimensions a 10.214(2), b 12.213(2), c 10.051(3) Å, α 79.53(2), β 105.25(2), γ 96.26(2)° and V 1187.2(5) Å3. Refinement was done to a final agreement for 3950 reflections with F023σ(F02) of R(F) = 0.042" @default.
- W2079160699 created "2016-06-24" @default.
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- W2079160699 date "1989-03-01" @default.
- W2079160699 modified "2023-10-17" @default.
- W2079160699 title "Some metallabicyclo-octadienes and -nonadienes of dicyclopentadienyltitanium, - zirconium and -hafnium" @default.
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- W2079160699 doi "https://doi.org/10.1016/0022-328x(89)87115-3" @default.
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