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• W2079183524 startingPage "3622" @default.
• W2079183524 abstract "The role of carbon additions and oxygen content on the densification of zirconium diboride ( ZrB 2 ) was studied. ZrB 2 with up to 1 wt% added carbon was hot pressed at temperatures of 2000°C and 2100°C. Nominally pure ZrB 2 hot pressed at 2100°C achieved relative densities >95.5%. Carbon and oxygen analysis indicate that oxygen removal was facilitated by the reduction of oxides with carbon or the removal of boria ( B 2 O 3 ) as a vapor. Therefore, by removing oxides from the particle surfaces, carbon additions of ≥0.5 wt% enabled densification to proceed to >96.5% of theoretical at 2000°C. Raman spectroscopy revealed the formation of boron carbide ( B 4.3 C ) in specimens with carbon additions of ≥0.75 wt%. The formation of B 4.3 C was eliminated via a 1 wt% addition of zirconium hydride ( ZrH 2 ), as a source of zirconium, resulting in the formation of carbon as the only residual second phase. Grain sizes were in the range of 7–10 μm (2000°C) and 12–16 μm (2100°C) and only appeared to be controlled by temperature, as no trends due to the evaluated carbon or oxygen contents were observed." @default.
• W2079183524 created "2016-06-24" @default.
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• W2079183524 date "2013-08-30" @default.
• W2079183524 modified "2023-10-02" @default.
• W2079183524 title "Effect of Carbon and Oxygen on the Densification and Microstructure of Hot Pressed Zirconium Diboride" @default.
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• W2079183524 doi "https://doi.org/10.1111/jace.12561" @default.
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